ASTM-D4273 Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols

ASTM-D4273 - 2023 EDITION - CURRENT
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Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols
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Scope

1.1 Carbon-13 Nuclear Magnetic Resonance Spectroscopy (13C NMR) measures the primary hydroxyl content of ethylene oxide (EO)-propylene oxide (PO) polyether polyols used in preparing flexible polyurethane foams. This method is best suited for polyether polyols with primary hydroxyl contents of 10 to 90 %.

1.2 The values stated in SI units are to be regarded as standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

Note 1: There is no known ISO equivalent to this standard.

1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Significance and Use

5.1 The primary hydroxyl content provides information about the relative reactivities of polyols in the urethane forming reaction with isocyanates.

Keywords

NMR; nuclear magnetic resonance spectroscopy; polyurethane raw materials; primary hydroxyl, polyether polyol;

To find similar documents by ASTM Volume:

08.02 (Plastics (II): D3222 - D5083)

To find similar documents by classification:

83.080.20 (Thermoplastic materials)

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Document Number

ASTM-D4273-23

Revision Level

2023 EDITION

Status

Current

Modification Type

Revision

Publication Date

March 15, 2023

Document Type

Test Method

Page Count

7 pages

Committee Number

D20.22