ASTM-D4273 › Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols
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Scope
1.1 Carbon-13 Nuclear Magnetic Resonance Spectroscopy (13C NMR) measures the primary hydroxyl content of ethylene oxide (EO)-propylene oxide (PO) polyether polyols used in preparing flexible polyurethane foams. This method is best suited for polyether polyols with primary hydroxyl contents of 10 to 90 %.
1.2 The values stated in SI units are to be regarded as standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Significance and Use
5.1 The primary hydroxyl content provides information about the relative reactivities of polyols in the urethane forming reaction with isocyanates.
Keywords
NMR; nuclear magnetic resonance spectroscopy; polyurethane raw materials; primary hydroxyl, polyether polyol;
To find similar documents by ASTM Volume:
08.02 (Plastics (II): D3222 - D5083)
To find similar documents by classification:
83.080.20 (Thermoplastic materials)
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Document Number
ASTM-D4273-23
Revision Level
2023 EDITION
Status
Current
Modification Type
Revision
Publication Date
March 15, 2023
Document Type
Test Method
Page Count
7 pages
Committee Number
D20.22