ASTM-D4291 Standard Test Method for Trace Ethylene Glycol in Used Engine Oil

ASTM-D4291 - 2021 EDITION - CURRENT
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Standard Test Method for Trace Ethylene Glycol in Used Engine Oil
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Scope

1.1 This test method covers the determination of ethylene glycol as a contaminant in used engine oil. This test method is designed to quantitate ethylene glycol in the range from 5 mass ppm to 200 mass ppm.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7.

Note 1: A qualitative determination of glycol-base antifreeze is provided in Test Methods D2982. Procedure A is sensitive to about 100 ppm.

1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Significance and Use

5.1 Leakage of aqueous engine coolant into the crank case weakens the ability of the oil to lubricate. If ethylene glycol is present, it promotes varnish and deposit formation. This test method is designed for early detection to prevent coolant from accumulating and seriously damaging the engine.

Keywords

antifreeze; ethylene glycol; gas chromatography; used engine oil;

To find similar documents by ASTM Volume:

05.02 (Petroleum Products and Lubricants (II): D3711 - D6122)

To find similar documents by classification:

75.100 (Lubricants, industrial oils and related products Including mineral oils, fluids for metal working and for temporary protection against corrosion Lubrication systems, see 21.260 Insulating oils, see 29.035.40)

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Document Number

ASTM-D4291-21

Revision Level

2021 EDITION

Status

Current

Modification Type

Revision

Publication Date

Dec. 21, 2021

Document Type

Test Method

Page Count

4 pages

Committee Number

D02.04.0L