ASTM-D6328 Standard Guide for Quality Assurance Protocols for Chemical Analysis of Atmospheric Wet Deposition

ASTM-D6328 - 2018 EDITION - CURRENT
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This guide describes quality assurance protocols for the determination of the anions and cations in atmospheric wet deposition which include the minimum recommended requirements for the preparation of calibration standards and suggested procedures for validating laboratory measurement results. Specimens to be used in all tests shall consist of reagent grade chemicals, water, and standard solutions. Common techniques for chemical analysis include automated colorimetry; ion chromatography, flame atomic absorption spectrophotometry, electrometry, and inductively coupled plasma spectrometry. Analytical precision and bias determinations shall be done for evaluation of the reference materials. Samples for reanalysis may be selected from the evaluation of control charts and the calculation of ion and conductivity percent differences.

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Scope

1.1 This guide describes quality assurance (QA) protocols for the determination of the anions and cations in Atmospheric Wet Deposition (AWD) shown in Table 1.

1.2 Included in this guide are minimum recommended requirements for the preparation of calibration standards and suggested procedures for validating laboratory measurement results.

1.3 This guide describes minimum requirements for the frequency of analysis of quality assurance samples and recommends procedures for the evaluation of quality assurance data.

1.4 The guide's recommendations are based upon expected anion and cation concentrations in AWD (1)2 and Appendix X1.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Keywords

atmospheric deposition; atomic absorption spectrophotometry; ion chromatography; quality assurance; quality control; wet deposition;; ICS Number Code 03.120.10 (Quality management and quality assurance); 13.040.20 (Ambient atmospheres); 71.040.40 (Chemical analysis)

To find similar documents by ASTM Volume:

11.07 (Atmospheric Analysis)

To find similar documents by classification:

03.120.10 (Quality management and quality assurance)

13.040.20 (Ambient atmospheres Including indoor air)

71.040.40 (Chemical analysis Including analysis of gases and surface chemical analysis)

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Document Number

ASTM-D6328-18

Revision Level

2018 EDITION

Status

Current

Modification Type

Revision

Publication Date

May 1, 2018

Document Type

Guide

Page Count

7 pages

Committee Number

D22.03