ASTM-D7214 Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation

ASTM-D7214 - 2023 EDITION - CURRENT
Show Complete Document History

Document Center Inc. is an authorized dealer of ASTM standards.
The following bibliographic material is provided to assist you with your purchasing decision:

Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation
ORDER

Price:

$63.00        


Want this as a site license?

Scope

1.1 This test method covers the determination of the oxidation of used lubricants by FT-IR (Fourier Transform Infrared Spectroscopy). It measures the concentration change of constituents containing a carbonyl function that have formed during the oxidation of the lubricant.

1.2 This test method may be used to indicate relative changes that occur in an oil under oxidizing conditions. The test method is not intended to measure an absolute oxidation property that can be used to predict performance of an oil in service.

1.3 This test method was developed for transmission oils which have been degraded either in service, or in a laboratory test, for example a bulk oxidation test. It may be used for other in-service oils, but the stated precision may not apply.

1.4 The results of this test method may be affected by the presence of other components with an absorbance band in the zone of 1600 cm-1 to 1800 cm-1. Low PAI values may be difficult to determine in those cases. Section 6 describes these possible interferences in more detail.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Significance and Use

5.1 The PAI is representative of the quantity of all the compounds containing a carbonyl function that have formed by the oxidation of the lubricant (aldehydes, ketones, carboxylic acids, esters, anhydrides, etc.). The PAI gives representative information on the chemical degradation of the lubricant which has been caused by oxidation.

5.2 This test method was developed for transmission oils and is used in the CEC L-48-A-00 test (Oxidation Stability of Lubricating Oils Used in Automotive Transmissions by Artificial Aging) as a parameter for the end of test evaluation.

Keywords

differential spectrum; FT-IR; in-service lubricant; lubricant; oxidation measurement; PAI; used oil;

To find similar documents by ASTM Volume:

05.03 (Petroleum Products and Lubricants (III): D6138 - D6971)

05.04 (Petroleum Products and Lubricants (IV): D6973 - latest)

To find similar documents by classification:

75.100 (Lubricants, industrial oils and related products Including mineral oils, fluids for metal working and for temporary protection against corrosion Lubrication systems, see 21.260 Insulating oils, see 29.035.40)

This document comes with our free Notification Service, good for the life of the document.

This document is available in either Paper or PDF format.

Document Number

ASTM-D7214-23

Revision Level

2023 EDITION

Status

Current

Modification Type

Revision

Publication Date

March 13, 2023

Document Type

Test Method

Page Count

7 pages

Committee Number

D02.96.03