SS-EN-ISO-18363-3 Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol (ISO 18363-3:2017)

SS-EN-ISO-18363-3 - 2021 EDITION - CURRENT


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This document specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3-MCPD esters (bound 3-MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis. This document is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.

To find similar documents by classification:

67.200.10 (Animal and vegetable fats and oils Butter, see 67.100.20)

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Designation Name

SS-EN ISO 18363-3:2021

Revision Level

2021 EDITION

Status

Current

Publication Date

Dec. 20, 2021

Language(s)

English

Page Count

32

International Equivalent

EN ISO 18363-3:2021(IDT); ISO 18363-3:2017(IDT)