ASTM-C1318 › Standard Test Method for Determination of Total Neutralizing Capability and Dissolved Calcium and Magnesium Oxide in Lime for Flue Gas Desulfurization (FGD)
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Scope
1.1 This test method covers analysis of magnesian, dolomitic and high-calcium limes for total neutralizing capability and dissolved major oxides. Dissolved calcium and magnesium are the major species that neutralize acid under the conditions of the test.
1.2 The test conditions are chosen to measure the acid-neutralizing capacity of both calcium hydroxide and magnesium hydroxide contained in slaked lime. By controlling the neutralization pH at 6, magnesium hydroxide and magnesium oxide are titrated in addition to calcium hydroxide fraction.
1.3 This test method also determines the fraction of Mg ions present in the lime that will dissolve under lime flue gas desulfurization (FGD) conditions. Because the Mg++ ion alters FGD performance, it is important to know its concentration.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Significance and Use
There are existing lime-based flue gas desulfurization units in operation that require a method to measure the oxides available for sulfur dioxide absorption. Dissolved magnesium oxide varies among limes depending on the limestone sources and calcination conditions.
Keywords
dissolved calcium; dissolved magnesium; flue gas desulfurization (FGD); lime; pH determination; total neutralizing capability; ICS Number Code 75.180.20 (Processing equipment)
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75.180.20 (Processing equipment)
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Document Number
ASTM-C1318-15AR20
Revision Level
2015A R20 EDITION
Status
Current
Publication Date
Jan. 13, 2021
Document Type
Test Method
Page Count
3 pages
Committee Number
C07.05