ASTM-D3268 › Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
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1.1 The sodium bicarbonate-coated glass tube and membrane filter method provides a means for the separation and collection of gaseous atmospheric forms of fluoride reactive with sodium bicarbonate and particulate forms of fluoride which are collected by a filter. The test method is applicable to 12-h sampling periods, collecting 1 to 500 μg of gaseous fluoride at a 15 L/min (0.5 ft3/min) sampling rate or about 0.1 to 50 μg/m3. The length of the sampling period can therefore be adjusted so that the amount of fluoride collected will fall within this range. The actual lower limit of the test method will depend upon the sensitivity of the analytical method employed and the quality of reagents used in tube preparation and analysis. It is recommended that the lower limit of detection should be considered as two times the standard deviation of the monthly arithmetic mean blank value. Any values greater than the blank by less than this amount should be reported as “blank value.”
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Significance and Use
5.1 The sodium bicarbonate coated tube filter method provides a means of separating and collecting atmospheric gaseous fluoride and particulate fluoride samples.
5.2 Since the samples are collected on the dry tube and filter, the fluoride may be eluted with a small volume of eluant (see Section for specific instructions on fluoride elution). Elution into a small volume and the sensitivity of the analytical methods employed allow the analysis of the collected fluoride to fractional parts of a microgram per cubic metre on samples taken for a 12-h period.
ambient atmospheres; analysis; fluoride; gaseous fluoride; particulate fluoride; sampling;; ICS Number Code 13.040.20 (Ambient atmospheres)
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1991 R18 EDITION
April 15, 2018