ASTM-D4222 › Standard Test Method for Determination of Nitrogen Adsorption and Desorption Isotherms of Catalysts and Catalyst Carriers by Static Volumetric Measurements
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Scope
1.1 This test method covers the determination of nitrogen adsorption and desorption isotherms of catalysts and catalyst carriers at the boiling point of liquid nitrogen.2 A static volumetric measuring system is used to obtain sufficient equilibrium adsorption points on each branch of the isotherm to adequately define the adsorption and desorption branches of the isotherm. Thirty points evenly spread over the isotherm is considered to be the minimum number of points that will adequately define the isotherm.
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Significance and Use
5.1 The test method has two main functions: first, it provides data useful for establishing the pore size distribution of catalyst materials, which in turn may influence their performance; and second, it serves as a laboratory test which may be used to study porosity changes that may occur during the manufacture and evaluation of catalysts.
Keywords
adsorption; catalysts; desorption; isotherms; nitrogen gas; volumetric;
To find similar documents by ASTM Volume:
05.05 (Combustion Characteristics; Manufactured Carbon and Graphite Products; Catalysts)
05.06 (Gaseous Fuels; Coal and Coke)
To find similar documents by classification:
71.040.30 (Chemical reagents Including reference materials)
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Document Number
ASTM-D4222-20
Revision Level
2020 EDITION
Status
Current
Modification Type
Revision
Publication Date
Nov. 3, 2020
Document Type
Test Method
Page Count
6 pages
Committee Number
D32.01