ASTM-D5953M Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection

ASTM-D5953M - 2016 EDITION - CURRENT
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Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection
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Scope

1.1 This test method2 presents a procedure for sampling and determination of non-methane organic compounds (NMOC) in ambient, indoor, or workplace atmospheres.

1.2 This test method describes the collection of integrated whole air samples in silanized or other passivated stainless steel canisters, and their subsequent laboratory analysis.

1.2.1 This test method describes a procedure for sampling in canisters at final pressures above atmospheric pressure (pressurized sampling).

1.3 This test method employs a cryogenic trapping procedure for concentration of the NMOC prior to analysis.

1.4 This test method describes the determination of the NMOC by the flame ionization detection (FID), without the use of gas chromatographic columns and other procedures necessary for species separation.

1.5 The range of this test method is from 20 to 10 000
ppb C (1, 2).3

1.6 This test method has a larger uncertainty for some halogenated or oxygenated hydrocarbons than for simple hydrocarbons or aromatic compounds. This is especially true if there are high concentrations of chlorocarbons or chlorofluorocarbons present.

1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

ambient atmospheres; analysis; atmospheres; canister sampling; cryogenic pre-concentration; flame ionization detection; indoor atmospheres; non-methane organic compounds; sampling; workplace atmospheres ;; ICS Number Code 13.040.01 (Air quality in general); 71.040.50 (Physicochemical methods of analysis)

To find similar documents by ASTM Volume:

11.07 (Atmospheric Analysis)

To find similar documents by classification:

13.040.01 (Air quality in general)

71.040.50 (Physicochemical methods of analysis Including spectrophotometric and chromatographic analysis)

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Document Number

ASTM-D5953M-16

Revision Level

2016 EDITION

Status

Current

Modification Type

Revision with Title Change

Publication Date

Oct. 15, 2016

Document Type

Test Method

Page Count

14 pages

Committee Number

D22.03