ASTM-D6595 Historical Revision Information
Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry

ASTM-D6595 - 2000 R11 EDITION - SUPERSEDED
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Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry
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Scope

1.1 This test method covers the determination of wear metals and contaminants in used lubricating oils and used hydraulic fluids by rotating disc electrode atomic emission spectroscopy (RDE-AES).

1.2 This test method provides a quick indication for abnormal wear and the presence of contamination in new or used lubricants and hydraulic fluids.

1.3 This test method uses oil-soluble metals for calibration and does not purport to relate quantitatively the values determined as insoluble particles to the dissolved metals. Analytical results are particle size dependent and low results may be obtained for those elements present in used oil samples as large particles.

1.4 The test method is capable of detecting and quantifying elements resulting from wear and contamination ranging from dissolved materials to particles approximately 10 m in size.

1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. The preferred units are mg/kg (ppm by mass).

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Significance and Use

Used Lubricating OilThe determination of debris in used oil is a key diagnostic method practiced in machine condition monitoring programs. The presence or increase in concentration of specific wear metals can be indicative of the early stages of wear if there are baseline concentration data for comparison. A marked increase in contaminant elements can be indicative of foreign materials in the lubricants, such as antifreeze or sand, which may lead to wear or lubricant degradation. The test method identifies the metals and their concentration so that trends relative to time or distance can be established and corrective action can be taken prior to more serious or catastrophic failure.

Keywords

additive elements; contaminant; disc electrode; emission spectrometry; lubricating oil; RDE; rod electrode; rotating disc electrode spectrometer; wear metal; ICS Number Code 75.100 (Lubricants, industrial oils and related products)

To find similar documents by ASTM Volume:

05.03 (Petroleum Products and Lubricants (III): D6138 - D6971)

To find similar documents by classification:

75.100 (Lubricants, industrial oils and related products Including mineral oils, fluids for metal working and for temporary protection against corrosion Lubrication systems, see 21.260 Insulating oils, see 29.035.40)

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Document Number

ASTM-D6595-00(2011)

Revision Level

2000 R11 EDITION

Status

Superseded

Modification Type

Reapproval

Publication Date

Aug. 15, 2011

Document Type

Test Method

Page Count

6 pages

Committee Number

D02.03