ASTM-D6869 Standard Test Method for Coulometric and Volumetric Determination of Moisture in Plastics Using the Karl Fischer Reaction (the Reaction of Iodine with Water)

ASTM-D6869 - 2017 EDITION - CURRENT
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Standard Test Method for Coulometric and Volumetric Determination of Moisture in Plastics Using the Karl Fischer Reaction (the Reaction of Iodine with Water)
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Scope

1.1 This method uses the reaction of Iodine (I2) with water (Karl Fischer Reaction) to determine the amount of moisture in a polymer sample.2

1.2 This test method is intended to be used for the determination of moisture in most plastics. Plastics containing volatile components such as residual monomers and plasticizers are capable of releasing components that will interfere with the I2/water reaction.

1.3 This method is suitable for measuring moisture over the range of 0.005 to 100 %. Sample size shall be adjusted to obtain an accurate moisture measurement.

1.4 The values stated in SI units are regarded as the standard.

Note 1: This standard is equivalent to ISO 15512 Method B.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Significance and Use

4.1 Moisture will affect the process ability of some plastics. High moisture content causes surface imperfections (that is, splay or bubbling) or degradation by hydrolysis. Low moisture (with high temperature) causes polymerization.

4.2 The physical properties of some plastics are affected by the moisture content.

Keywords

moisture content; moisture determination; plastics;

To find similar documents by ASTM Volume:

08.03 (Plastics (III): D5117 - latest; Reinforced Plastic Piping Systems and Chemical Equipment; Plastic Building Products)

To find similar documents by classification:

83.080.01 (Plastics in general)

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Document Number

ASTM-D6869-17

Revision Level

2017 EDITION

Status

Current

Modification Type

Revision

Publication Date

Dec. 1, 2017

Document Type

Test Method

Page Count

4 pages

Committee Number

D20.70