ASTM-D7245 Standard Test Method for Measuring Total Water and Volatiles in Liquid Coatings Which Produce Cure Water Upon Heating

ASTM-D7245 - 2009 R21 EDITION - CURRENT
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Standard Test Method for Measuring Total Water and Volatiles in Liquid Coatings Which Produce Cure Water Upon Heating
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Scope

1.1 This test method is designed to measure total water which includes cure water resulting from the heat induced condensation reaction of coatings. Cure water cannot be measured directly by Test Method D 4017. This task is accomplished by measuring water content in the vapors evolved during heating. This test method will yield total water content. This test method also permits for the simultaneous determination of total volatile content. The results of this test method may be used to calculate VOC content. Although this test method was designed for phenolic coatings, it can be used with other types of coatings.

1.2 Materials used for method development and evaluation had total water values from 20 to 37 %. Use of this test method on coatings outside these values will need to be validated by the user.

1.3 Sample heating is accomplished with a Brinkmann Instruments Model 832 drying oven, or other mutually agreed upon alternative, passing all of the evolved vapors into a Karl Fischer titration vessel.

1.4 &solely-SI-units;

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Significance and Use

In the determination of VOC, cure water is treated as a VOC in other test methods, as these methods are unable to account for cure water. This test method allows taking credit for cure water as total water is measured, a value which includes cure water.

Total water content and volatile content results obtained with this method may be used in Practice D 3960 to calculate VOC of the coating.

Keywords

condensation reaction; cure water; drying oven; Karl Fischer; total water; VOC ; volatile; volatile organic content; ICS Number Code 87.040 (Paints and varnishes)

To find similar documents by ASTM Volume:

06.01 (Paint -- Tests for Chemical, Physical, and Optical Properties; Appearance)

To find similar documents by classification:

87.040 (Paints and varnishes Including coating powders, paint coatings and protective paint systems)

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Document Number

ASTM-D7245-09R21

Revision Level

2009 R21 EDITION

Status

Current

Modification Type

New

Publication Date

March 3, 2021

Document Type

Test Method

Committee Number

D01.21