ASTM-E2402 Standard Test Method for Mass Loss, Residue, and Temperature Measurement Validation of Thermogravimetric Analyzers

ASTM-E2402 - 2019 EDITION - CURRENT
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Standard Test Method for Mass Loss, Residue, and Temperature Measurement Validation of Thermogravimetric Analyzers
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Scope

1.1 This test method provides procedures for validating mass loss, residue, and temperature measurements by thermogravimetric analyzers (TGAs) and analytical methods based upon the measurement of mass loss or residue content or temperature. Performance parameters determined include mass loss, residue, and temperature repeatability (precision), detection limit, quantitation limit, linearity, and bias.

1.2 Validation of apparatus performance and analytical methods is requested or required for quality initiatives or where results may be used for legal purposes.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Significance and Use

5.1 This test method may be used to validate the performance of a specific thermogravimetric analyzer.

5.2 This test method may be used to validate the performance of a specific method based upon a thermogravimetry mass loss or residue measurement.

5.3 This test method may be used to determine the repeatability of a specific apparatus, operator, or laboratory.

5.4 This test method may be used for specification and regulatory compliance purposes.

Keywords

detection limit; linearity; precision; quantitation limit; range; repeatability; thermal analysis; thermogravimetric analysis; validation;

To find similar documents by ASTM Volume:

14.02 (General Test Methods; Forensic Psychophysiology; Forensic Sciences; Terminology; Conformity Assessment; Statistical Methods; Nanotechnology; Forensic Engineering; Manufacture of Pharmaceutical Products)

To find similar documents by classification:

19.020 (Test conditions and procedures in general)

71.040.10 (Chemical laboratories. Laboratory equipment Including hydrometers, alcoholometers, etc. Apparatus for measurement of volume, mass, density, viscosity, see 17.060 Spectroscopes, see 17.180.30 Temperature-measuring instruments, see 17.200.20 Laboratory ware, see 71.040.20)

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Document Number

ASTM-E2402-19

Revision Level

2019 EDITION

Status

Current

Modification Type

Revision with Title Change

Publication Date

Sept. 1, 2019

Document Type

Test Method

Page Count

7 pages

Committee Number

E37.10