ISO-2272 › Surface active agents -- Soaps -- Determination of low contents of free glycerol by molecular absorption spectrometry
ISO-2272
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2ND EDITION
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CURRENT
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The determination is carried out in the following way: Decomposition of the soap by sulfuric acid and extraction of the fatty acida with light petroleum. Oxidation of the free glycerol remaining in the aqueous phase by periodic acid to formic acid and formaldehyde. On reaction with chromotropic acid, the aldehyde formed gives an absorbing compound whose absorbance is propotional to the free glycerol content. Spectrometric measurement of the absorbance at a wavelength about 571 mm.
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71.100.40 (Surface active agents)
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Document Number
ISO 2272:1989
Revision Level
2ND EDITION
Status
Current
Publication Date
July 15, 1989
Committee Number
ISO TC 91