ASTM-D2868 Historical Revision Information
Standard Test Method for Nitrogen Content (Kjeldahl) and Hide Substance Content of Leather

ASTM-D2868 - 2010 EDITION - SUPERSEDED
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Standard Test Method for Nitrogen Content (Kjeldahl) and Hide Substance Content of Leather, Wet Blue and Wet White
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Scope

1.1 This test method covers the determination of the nitrogen content of all types of leather, wet blue and wet white. The nitrogen content is used to calculate the hide substance (protein fiber) content of leather, wet blue and wet white.

Note 1—The original test method for leather was essentially a composite of Method 6441 of Federal Test Method Standard No. 311 and Method B5 of the American Leather Chemists Association.

Note 2—Melamine, if present in bonded leather, could give an artificially high value for the calculation of protein fiber.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Significance and Use

The nitrogen content as determined by this test method is normally considered to be related to the amount of hide substance (protein fiber) present in the leather sample. A factor of 5.62 is normally used to calculate the hide substance from the nitrogen content.

The 5.62 factor represents the average result of many analyses of animal hides, but it cannot be considered to be accurate since it varies somewhat from hide to hide of the same type, from type of hide to type of hide, and also with the thickness of hide retained in the final leather (split thickness as compared to original hide thickness). As a result of these variations, the true factor for any given leather may be expected to vary from 5.44 to 5.80 or about ±3 %.

A given leather sample may contain nitrogenous substances other than hide substance (protein fiber) which will be analyzed for by this test method, such as resins, dyestuffs, etc., that contain nitrogen. Therefore, although this test method is fairly accurate for determining the nitrogen content of leather, its use for determining hide substance may result in large errors.

The hide substance value derived from this determination has a large bearing on other chemical determinations of a given leather. Any errors, such as those described in 4.1.1 and 4.2, will be carried over into these other analytical calculations.

Keywords

hide substance; Kjeldahl; nitrogen ; wet blue; wet white; Hide; Kjeldahl method; Leather; Nitrogen content; ICS Number Code 59.140.30 (Leather and furs)

To find similar documents by ASTM Volume:

15.04 (Soaps and Other Detergents; Polishes; Leather; Resilient Floor Coverings)

To find similar documents by classification:

59.140.30 (Leather and furs)

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Document Number

ASTM-D2868-10

Revision Level

2010 EDITION

Status

Superseded

Modification Type

Revision

Publication Date

Nov. 1, 2010

Document Type

Test Method

Page Count

5 pages

Committee Number

D31.06