ASTM-D4239 Historical Revision Information
Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion Methods

ASTM-D4239 - 2008 EDITION - SUPERSEDED
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Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion
ORDER

Scope

1.1 These test methods cover two alternative procedures using high-temperature tube furnace combustion methods for the rapid determination of sulfur in samples of coal and coke.

1.2 These test methods appear in the following order:

Sections
Method AHigh-Temperature Combustion Method with Acid Base Titration Detection Procedures6-9
Method BHigh-Temperature Combustion Method with Infrared Absorption Detection Procedures10-12

Note 1—High Temperature Combustion Method with Iodimetric Detection procedures, formally Method B in the 2000 version of this standard is still a viable method that may be used.

1.2.1 When automated equipment is used to perform any of the two methods of this test method, the procedures can be classified as instrumental methods. There are several manufacturers that offer to the coal industry equipment with instrumental analysis capabilities for the determination of the sulfur content of coal and coke samples.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 7.7 and 11.2.

Significance and Use

p>Determination of sulfur is, by definition, part of the ultimate analysis of coal.

Results of the sulfur analysis are used to serve a number of interests: evaluation of coal preparation, evaluation of potential sulfur emissions from coal combustion or conversion processes, and evaluation of the coal quality in relation to contract specifications, as well as other scientific purposes.

The instrumental analysis provides a reliable, rapid method for determining the concentration of sulfur in a lot of coal or coke and are especially applicable when results must be obtained rapidly for the successful completion of industrial, beneficiation, trade, or other evaluations.

Keywords

Coal/coke products; Coke; Combustion; Furnaces; Sulfur--coal/coke; Temperature tests--coal/coke

To find similar documents by ASTM Volume:

05.06 (Gaseous Fuels; Coal and Coke)

To find similar documents by classification:

75.160.10 (Solid fuels Including coal products, coke, peat, wood, derivatives of coal pyrolysis, etc. Coals, see 73.040)

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Document Number

ASTM-D4239-08

Revision Level

2008 EDITION

Status

Superseded

Modification Type

Revision

Publication Date

Feb. 1, 2008

Document Type

Test Method

Page Count

8 pages

Committee Number

D05.21