ASTM-D6042 › Historical Revision Information
Standard Test Method for Determination of Phenolic Antioxidants and Erucamide Slip Additives in Polypropylene Homopolymer Formulations Using Liquid Chromatography (LC)
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Scope
1.1 This test method covers a liquid-chromatographic procedure for the separation of some additives currently used in polypropylene. These additives are extracted with a cyclohexane:methylene chloride mixture using either reflux or ultrasonic bath prior to liquid-chromatographic separation. The ultraviolet absorbence (200 nm) of the compound(s) is measured, and quantitation is performed using the internal standard method.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.
Note 1- There is no similar or equivalent ISO standard.
Keywords
additive; antioxidants; erucamide slip; extraction; Irgafos 168; Irganox 1010; Irganox 1076; Irganox 3114; liquid chromatography (LC); polypropylene (PP); vitamin E; ICS Number Code 71.040.50 (Physicochemical methods of analysis); 83.080.20 (Thermoplastic materials)
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83.080.20 (Thermoplastic materials)
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Document Number
ASTM-D6042
Revision Level
WITHDRAWN
Status
Superseded
Modification Type
New
Publication Date
Jan. 1, 2009
Document Type
Test Method
Committee Number
D20.70