ASTM-D6301 Historical Revision Information
Standard Practice for Collection of On-Line Composite Samples of Suspended Solids and Ionic Solids in Process Water

ASTM-D6301 - 2013 EDITION - SUPERSEDED
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Standard Practice for Collection of On-Line Composite Samples of Suspended Solids and Ionic Solids in Process Water
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Scope

1.1 This practice is applicable for sampling condensed steam or water, such as boiler feedwater, for the collection of suspended solids and (optional) ionic solids using a 0.45-μm membrane filter (suspended solids) and ion exchange media (ionic solids). As the major suspended component found in most boiler feedwaters is some form of corrosion product from the preboiler system, the device used for this practice is commonly called a corrosion product sampler.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Significance and Use

5.1 The transport of any suspended solids or corrosion products from the preboiler cycle has been shown to be detrimental to all types of steam generating equipment. Corrosion product transport as low as 10 ppb can have significant impact on steam generators performance.

5.2 Deposited corrosion products on PWR steam generator tubes can reduce heat transfer, and, if the deposit is sufficiently thick, can provide a local area for impurities in the bulk water to concentrate, resulting in a corrosive environment. In BWR plants, the transport of corrosion products can cause fuel failure, out of core radiation problems from activation reactions, and other material related problems.

5.3 In fossil plants, the transport of corrosion products can reduce heat transfer in the boilers leading to tube failures from overheating. The removal of these corrosion products by chemical cleaning is expensive and potentially harmful to the boiler tubes.

5.4 Normally, grab samples are not sensitive enough to detect changes in the level of corrosion product transport. Also, system transients may be missed by only taking grab samples. An integrated sample over time will increase the sensitivity for detecting the corrosion products and provide a better understanding of the total corrosion product transport to steam generators.

Keywords

corrosion products; corrosion product sampler; filtration; integrated sample; ion exchange membranes

To find similar documents by ASTM Volume:

11.01 (Water (I))

To find similar documents by classification:

13.060.45 (Examination of water in general Including sampling)

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Document Number

ASTM-D6301-13

Revision Level

2013 EDITION

Status

Superseded

Modification Type

Revision

Publication Date

Aug. 15, 2013

Document Type

Practice

Page Count

5 pages

Committee Number

D19.03