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1.1 This test method covers the microscopical determination of the reflectance measured in immersion oil of polished surfaces of vitrinite dispersed in sedimentary rocks. This test method can also be used to determine the reflectance of macerals other than vitrinite dispersed in sedimentary rocks.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

5.1 The mean reflectance of the vitrinite maceral in sedimentary rocks as determined by this test method is used as an indicator of thermal maturity, that is, the progressive geochemical alteration of dispersed organic material experienced during diagenesis, catagenesis, and metagenesis. In the case of hydrocarbon source rocks, three major categories of thermal maturity are defined by vitrinite reflectance: immature (R_oran ≤ 0.5 %), mature (R_oran ≈ 0.5 % to 1.35 %), and overmature (R_oran ≥ 1.35 %) with respect to the generation of liquid hydrocarbons, although not all practitioners agree on these thermal boundaries (10). Thermal maturity as determined by the reflectance of vitrinite dispersed in sedimentary rocks is similar to the rank classification of coals as presented in Classification D388 and measured similarly to the reflectance of vitrinite in coal as presented in Test Method D2798. The mean reflectance of the vitrinite maceral in sedimentary rocks correlates with geochemically determined parameters of thermal maturity and can be used to characterize thermal maturation history, to calibrate burial history models, and to better understand the processes of hydrocarbon generation, migration, and accumulation in conventional and unconventional petroleum systems.