ASTM-B822 Standard Test Method for Particle Size Distribution of Metal Powders and Related Compounds by Light Scattering

ASTM-B822 - 2017 EDITION - CURRENT
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Standard Test Method for Particle Size Distribution of Metal Powders and Related Compounds by Light Scattering
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Scope

1.1 This test method covers the determination of the particle size distribution by light scattering, reported as volume percent, of particulate materials including metals and compounds.

1.2 This test method applies to analyses with both aqueous and nonaqueous dispersions. In addition, analysis can be performed with a gaseous dispersion for materials that are hygroscopic or react with a liquid carrier.

1.3 This test method is applicable to the measurement of particulate materials in the range of 0.4 to 2000 μm, or a subset of that range, as applicable to the particle size distribution being measured.

1.4 The values stated in SI units are to be regarded as the standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Significance and Use

5.1 Reported particle size measurement is a function of both the actual particle dimension and shape factor as well as the particular physical or chemical properties being measured. Caution is required when comparing data from instruments operating on different physical or chemical parameters or with different particle size measurement ranges. Sample acquisition, handling, and preparation can also affect reported particle size results.

5.1.1 It is important to recognize that the results obtained by this test method, or any other method for particle size determination using different physical principles, may disagree. The results are strongly influenced by the physical principles employed by each method of particle size analysis. The results of any particle sizing method should be used only in a relative sense; they should not be regarded as absolute when comparing results obtained by other methods.

5.2 Light scattering theory has been available for many years for use in the determination of particle size. Several manufacturers of testing equipment now have units based on these principles. Although each type of testing equipment uses the same basic principles for light scattering as a function of particle size, different assumptions pertinent to application of the theory, and different models for converting light measurements to particle size, may lead to different results for each instrument. Therefore, the use of this test method cannot guarantee directly comparable results from different types of instruments.

5.3 Knowledge of the particle size distribution of metal powders is useful in predicting the powder-processing behavior and ultimate performance of powder metallurgy parts. Particle size distribution is related closely to the flowability, moldability, compressibility, and die-filling characteristics of a powder, as well as to the final structure and properties of finished powder metallurgy (P/M) parts.

5.4 This test method is useful to both suppliers and users of powders in determining the particle size distributions for product specifications, manufacturing control, development, and research.

5.5 This test method may be used to obtain data for comparison between lots of the same material or for establishing conformance, as in acceptance testing.

Keywords

laser diffraction; light scattering; metal powders; particle size distribution; powder metallurgy ;; ICS Number Code 13.300 (Protection against dangerous goods)

To find similar documents by ASTM Volume:

02.05 (Metallic and Inorganic Coatings; Metal Powders and Metal Powder Products)

To find similar documents by classification:

13.300 (Protection against dangerous goods Including performance requirements for dangerous goods, their handling, storage, transportation, marking, labelling, etc. Nuclear fissile materials, see 27.120.30 Explosives, see 71.100.30)

19.120 (Particle size analysis. Sieving Including test sieves and porosimetry)

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Document Number

ASTM-B822-17

Revision Level

2017 EDITION

Status

Current

Modification Type

Revision

Publication Date

May 1, 2017

Document Type

Test Method

Page Count

4 pages

Committee Number

B09.02