ASTM-D4273 › Historical Revision Information
Standard Test Method for Polyurethane Raw Materials: Determination of Primary Hydroxyl Content of Polyether Polyols
The following bibliographic material is provided to assist you with your purchasing decision:
Scope
1.1 Carbon-13 Nuclear Magnetic Resonance Spectroscopy (carbon-13 NMR), measures the primary hydroxyl content of ethylene oxide-propylene oxide polyethers used in preparing flexible foams. It is best suited for polyethers with primary hydroxyl contents of 10 to 90 %.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1—There is no known ISO equivalent to this standard.
X1.1.1 Fluorine-19 Nuclear Magnetic Resonance Spectroscopy (fluorine-19 NMR), measures the primary hydroxyl content in ethylene oxide-propylene oxide polyethers used in flexible urethane foams. It is suitable for polyethers with hydroxyl numbers of 24 to 300 and primary hydroxyl percentages of 2 to 98.
Significance and Use
Measurements of primary hydroxyl content are useful for providing information regarding the relative reactivities of polyols.
Keywords
NMR; nuclear magnetic resonance spectroscopy; polyurethane raw materials; primary hydroxyl, polyether polyol; Hydroxyl (hydroxide ion) content; Nuclear magnetic resonance (NMR) spectrometry; Polyether polyols; Polyols; Polyurethane insulation; Polyurethane raw materials--polyols; ICS Number Code 83.080.20 (Thermoplastic materials)
To find similar documents by ASTM Volume:
08.02 (Plastics (II): D3222 - D5083)
To find similar documents by classification:
83.080.20 (Thermoplastic materials)
This document comes with our free Notification Service, good for the life of the document.
This document is available in either Paper or PDF format.
Document Number
ASTM-D4273-11
Revision Level
2011 EDITION
Status
Superseded
Modification Type
Revision
Publication Date
April 1, 2011
Document Type
Test Method
Page Count
8 pages
Committee Number
D20.22