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Scope

1.1 This test method is for the determination of the inherent viscosity of poly(ethylene terephthalate) (PET) soluble at 0.50 % concentration in a 60/40 phenol/1,1,2,2-tetrachloroethane solution by means of a glass capillary viscometer. Highly crystalline forms of PET that are not soluble in this solvent mixture will require a different procedure.

1.2 The inherent viscosity values obtained by this test method are comparable with those obtained using differential viscometry described in Test Method D5225.

1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 8.

Note 1—This test method and ISO 1628-5 are similar but not technically equivalent. This ISO standard gives an option of solvents for PET. Solvent specified in this ASTM test method is one of the options in the ISO method. ISO also uses Type 1C Ubbelohde viscometer, rather than the 1B, and reports viscosity number, rather than inherent viscosity.

Significance and Use

The inherent viscosity is relatable to the composition and molecular weight of a polyester resin. It must be controlled so that the processability and end properties of the resin remain in a desired range.

Keywords

glass capillary viscometer; inherent viscosity; poly(ethylene terephthalate); PET; solution viscosity; Flow and flow rate--thermoplastics; Glass capillary viscometer; PET (poly(ethylene terephthalate)); Polymer content; Viscosity--plastics; ICS Number Code 83.080.20 (Thermoplastic materials)

To find similar documents by ASTM Volume:

08.02 (Plastics (II): D3222 - D5083)

08.03 (Plastics (III): D5117 - latest; Reinforced Plastic Piping Systems and Chemical Equipment; Plastic Building Products)

To find similar documents by classification:

83.080.20 (Thermoplastic materials)

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