ASTM-D7365 › Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
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Scope
1.1 This practice is applicable for the collection and preservation of water samples for the analysis of cyanide. This practice also addresses the mitigation of known interferences prior to the analysis of cyanide.
1.2 The sampling, preservation and mitigation of interference procedures described in this practice are recommended for the analysis of total cyanide, available cyanide, weak acid dissociable cyanide, and free cyanide by Test Methods D 2036, D 4282, D 4374, D 6888, D 6994, and D 7237. This practice can also be applied to other cyanide methods, for example, US EPA Method 335.4 and Standard Methods 4500-CN- C.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Significance and Use
Cyanide is routinely analyzed in water samples, often to demonstrate regulatory compliance; however, improper sample collection or pretreatment can result in significant positive or negative bias potentially resulting in unnecessary permit violations or undetected cyanide releases into the environment.
Keywords
available cyanide; cyanide; free cyanide; hydrogen cyanide; interference; preservative; sample collection; total cyanide; ICS Number Code 13.060.50 (Examination of water for chemical substances)
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13.060.50 (Examination of water for chemical substances)
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Document Number
ASTM-D7365-09AR22
Revision Level
2009A R22 EDITION
Status
Current
Modification Type
New
Publication Date
May 13, 2022
Document Type
Practice
Page Count
11 pages
Committee Number
D19.06