ASTM-D8064 Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams

ASTM-D8064 - 2016 EDITION - CURRENT


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Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams
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Scope

1.1 This test method is based upon energy-dispersive X-ray Fluorescence (EDXRF) spectrometry using multiple monochromatic excitation beams for detection and quantification of selected heavy metal elements in soil and related solid waste.

1.2 This test method is also known as High Definition X-ray Fluorescence (HDXRF) or Multiple Monochromatic Beam EDXRF (MMB-EDXRF).

1.3 This test method is applicable to various soil matrices for the determination of Cr, Ni, As, Cd, Hg, and Pb in the range of 1 to 5000 mg/kg, as specified in Table 1 and determined by a ruggedness study using representative samples. The limit of detection (LOD) for each element is listed in Table 1. The LOD is estimated by measuring a SiO2 blank sample (see Table X1.1 in Appendix X1).

1.4 This test method is applicable to other elements: Sb, Cu, Se, Ag, Tl, Zn, Ba, Au, Co, V, Fe, Mn, Mo, K, Rb, Sn, Sr, and Ti.

1.5 X-ray Nomenclature—This standard names X-ray lines using the Siegbahn convention.2

1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

arsenic; As; cadmium; Cd; chromium; Cd; EDXRF; fundamental parameters; FP; HDXRF; heavy metals; Hg; lead; mercury; MMB-EDXRF; Multiple Monochromatic Beam EDXRF; Ni; nickel; Pb; soil; solid waste;; ICS Number Code 13.030.10 (Solid wastes); 13.080.05 (Examination of soils in general)

To find similar documents by ASTM Volume:

11.04 (Waste Management)

To find similar documents by classification:

13.030.10 (Solid wastes)

13.080.05 (Examination of soils in general Including sampling)

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Document Number

ASTM-D8064-16

Revision Level

2016 EDITION

Status

Current

Modification Type

New

Publication Date

Dec. 1, 2016

Document Type

Test Method

Page Count

12 pages

Committee Number

D34.01.06